Fourier Transform Infrared Spectroscopy (FT-IR) is a popular tool for determining
unknown identification and functional group presence in chemical systems. Impact
Analytical has a Thermo-Nicolet Nexus series bench driven by the Nicolet Omnic
software, as well as a Nicolet NicPlan IR microscope. The system includes library
searching capability and many operator help functions to simplify use of the
instrument.
Sampling formats include: KBr pellet, mull cells, and liquid cells, all of which
can be run at variable controlled temperature. Diamond ATR accessory is also
available.
Examples
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Because IR absorption is dependent upon a dipole moment change during each
molecular vibration and/or molecular rotation, functional group analysis as
well as molecular characterization and identification is possible. Researchers
involved in synthesis use the instrument frequently to determine if desired
functional groups are present in compounds they have synthesized.
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The system includes a polymers and additives library. A customer desiring
identification of a polymer used to mold a finished product submitted a sample
for unknown identification. A small amount of the polymer was excised from the
article and dissolved in a solvent. A thin film of the polymer was cast and its
infrared spectrum was measured. By searching the library, a match was found for
the spectrum thereby identifying the material.