Industrial and commercial tubing may be comprised of layers, dependent upon the
final tubing application. In this application, the different layers provide
discreet properties dictated by the environment to which each of the layers will
be exposed. The FT-IR microscopic technique may be used to characterize the
individual layers of the tubing.
Example:
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Multilayer tubing used for fuel applications was prepared for light microscopy
and infrared microscopy by cutting 10 and 15-micron thick sections on a
microtome using a diamond knife. The sections were imaged in a compound light
microscope fitted with a digital camera. Layer thickness was determined by use
of a micrometer photographed using the same settings as the tubing layers.
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The tubing sections were placed under the infrared objective of a Thermo-Nicolet
NicPlan® IR microscope. The image was centered and an aperture mask used so
that only the layer of interest was visible. In this way, a transmission
spectrum was obtained of each layer of each piece of tubing.